Overestimate of ESDs from Pilatus detector

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Andrew
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Overestimate of ESDs from Pilatus detector

#1 Post by Andrew » 2012.05.17 07:27

I have synchrotron SAXS that was collected off a Pilatus detector. The data are very nice, but the Chi values for a scattering curves regularised using Gnom is typically ~0.5, suggesting that the ESD are on average overestimated by a factor of ~2. Similar data collected from a Bruker NanoStar using their VANTEC detector yields values ~0.9.

Is it something inherent in the detector (Maybe the Gain of the detector needs correcting for), or is it likely that the data reduction is doing something a little strange?

It isn't a huge issue, but a reviewer is questioning the quality of our data based on the error bars (which are overestimated). I don't like arbitrarily scaling ESD's as I don't know whether the effect is independent of q or intensity. I would like an explanation that I give in the responses.

Andrew
Active member
Posts: 23
Joined: 2009.01.28 00:06

Re: Overestimate of ESDs from Pilatus detector

#2 Post by Andrew » 2012.06.08 02:43

It turns out that the data reduction program was outputting 2 standard errors, and I was assuming it was 1 standard error.

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